求翻译,希望大家帮忙.不要工具翻的,谢谢啦!
In a flask fitted with a reflux condenser were added 1.00 g
(10.4 mmol) of 1,2-dimethylimidazole and 1.43 g (10.4 mmol)
of butyl bromide. After addition, the mixture was stirred at
140 ◦C during 1 h to give a white solid. This solid was recrystallized
from acetonitrile and dried under reduced pressure to give
2.29 g (95% yield) of BMMIBr as white crystals. In another
flask, 250 mg (1.07 mmol) of BMMIBr were placed and dissolved
in 5.0mL of water followed by an aqueous solution
of LiTFSI (308 mg, 1.07 mmol) in 5.0mL of water. The reaction
mixture was stirred overnight at room temperature and two
phases were formed and separated. The phase containing the
ionic liquid was washed several times with water, treated with
activated carbon and subjected to a chromatography column
(alumina, dichloromethane). The ionic liquid was dried under
reduced pressure during 3 days at 100 ◦C to give BMMITFSI as
答案
在一个瓶子带有回流冷凝器增加了一点○○克（ 10.4 mmol ） 1,2 -d imethylimidazole和一点四三克（ 1 0.4m mol） 丁基溴化.之后,此外,混合搅拌,在140 ◦ c在1 h后给予一个白色固体.这是固体结晶从乙腈和干果的...
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